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Quenching of High Entropy Alloys after Annealing
(2020)
The effect of cooling rate after annealing at 900 °C on the microstructure and hardness of high entropy alloys was investigated using two typical samples with the chemical composition of Co₁₆Cr₁₄.₅Fe₂₉Mn₁₁.₅Ni₂₉ and Co₁₁.₅Cr₇Fe₂₇Mn₂₇Ni₂₇(Nb₀.₀₈C₀.₅) (at%). The microstructural characterisation and hardness measurements were carried out by optical microscopy, scanning electron microscopy, wavelength-dispersive X-ray spectroscopy, electron back scattered diffraction, X-ray diffraction technique and Vickers hardness ...
Aufsatz
Predicting Flow Stress Behavior of an AA7075 Alloy Using Machine Learning Methods
(2022-09-09)
The present work focuses on the prediction of the hot deformation behavior of thermo-mechanically processed precipitation hardenable aluminum alloy AA7075. The data considered focus on a novel hot forming process at different tool temperatures ranging from 24°C to 350°C to set different cooling rates after solution heat-treatment. Isothermal uniaxial tensile tests in the temperature range of 200°C to 400°C and at strain rates ranging from 0.001 s-¹ to 0.1 s-¹ were carried out on four different material conditions. ...
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Exploring the mechanical properties of additively manufactured carbon-rich zirconia 3D microarchitectures
(2023-07-11)
Two-photon lithography (TPL) is a promising technique for manufacturing ceramic microstructures with nanoscale resolution. The process relies on tailor-made precursor resins rich in metal–organic and organic constituents, which can lead to carbon-based residues incorporated within the ceramic microstructures. While these are generally considered unwanted impurities, our study reveals that the presence of carbon-rich residues in the form of graphitic and disordered carbon in tetragonal (t-) ZrO₂ can benefit the ...
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Influence of Cu Addition and Microstructural Configuration on the Creep Resistance and Mechanical Properties of an Fe-Based α/α′/α″ Superalloy
(2023-01-14)
Introducing Cu nanoparticles is an effective mechanism for strengthening and toughening Fe-based materials such as ultra-high-strength steels. Herein, the effect of Cu on the mechanical properties of a novel Fe-based α/α′/α″ superalloy is studied. Compared to a Cu-free reference alloy, nanoindentation reveals an increase in hardness, which was associated with the formation of Cu nanoparticles. Both alloys show room temperature (RT) compressive plastic strain at maximum stress greater than 8%, irrespective of the ...
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Additive Manufacturing of 3D Luminescent ZrO2:Eu3+ Architectures
(2022-04-27)
Implementation of more refined structures at the nano to microscale is expected to advance applications in optics and photonics. This work presents the additive manufacturing of 3D luminescent microarchitectures emitting light in the visible range. A tailor-made organo-metallic resin suitable for two-photon lithography is developed, which upon thermal treatment in an oxygen-rich atmosphere allows the creation of silicon-free tetragonal (t-) and monoclinic (m-) ZrO₂. The approach is unique because the tailor-made ...
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Structural reorientation and compaction of porous MoS₂ coatings during wear testing
(2022-04-02)
Industrial upscaling frequently results in a different coating microstructure than the laboratory prototypes presented in the literature. Here, we investigate the wear behavior of physical vapor deposited (PVD) MoS2 coatings: A dense, nanocrystalline MoS2 coating, and a porous, prismatic-textured MoS2 coating. Transmission electron microscopy (TEM) investigations before and after wear testing evidence a crystallographic reorientation towards a basal texture in both samples. A basal texture is usually desirable due ...
Aufsatz
Microcantilever Fracture Tests of α-Cr Containing NiAl Bond Coats
(2022-01-08)
MCrAlY bond coats are widely used as oxidation-resistant coatings on superalloys. The major phase is the thermally stable intermetallic β-NiAl phase. The addition of Cr increases the oxidation and corrosion resistance but leads to the formation of α-Cr precipitates. Both phases are brittle and limit the fracture toughness of these coatings. To study the influence of thermal exposure and the resulting changing chemical composition on the fracture properties, the fracture toughness of both phases is measured by notched ...