Suche
Anzeige der Dokumente 21-28 von 28
Aufsatz
Additive Manufacturing of 3D Luminescent ZrO2:Eu3+ Architectures
(2022-04-27)
Implementation of more refined structures at the nano to microscale is expected to advance applications in optics and photonics. This work presents the additive manufacturing of 3D luminescent microarchitectures emitting light in the visible range. A tailor-made organo-metallic resin suitable for two-photon lithography is developed, which upon thermal treatment in an oxygen-rich atmosphere allows the creation of silicon-free tetragonal (t-) and monoclinic (m-) ZrO₂. The approach is unique because the tailor-made ...
Aufsatz
Structural reorientation and compaction of porous MoS₂ coatings during wear testing
(2022-04-02)
Industrial upscaling frequently results in a different coating microstructure than the laboratory prototypes presented in the literature. Here, we investigate the wear behavior of physical vapor deposited (PVD) MoS2 coatings: A dense, nanocrystalline MoS2 coating, and a porous, prismatic-textured MoS2 coating. Transmission electron microscopy (TEM) investigations before and after wear testing evidence a crystallographic reorientation towards a basal texture in both samples. A basal texture is usually desirable due ...
Aufsatz
Microcantilever Fracture Tests of α-Cr Containing NiAl Bond Coats
(2022-01-08)
MCrAlY bond coats are widely used as oxidation-resistant coatings on superalloys. The major phase is the thermally stable intermetallic β-NiAl phase. The addition of Cr increases the oxidation and corrosion resistance but leads to the formation of α-Cr precipitates. Both phases are brittle and limit the fracture toughness of these coatings. To study the influence of thermal exposure and the resulting changing chemical composition on the fracture properties, the fracture toughness of both phases is measured by notched ...
Aufsatz
Investigation of processing windows in additive manufacturing of AlSi10Mg for faster production utilizing data-driven modeling
(2022-04-29)
To reduce production time and decrease production cost, the increase of layer thickness is an adequate option in powder bed fusion. In order to determine the relationships between process parameters in laser powder bed fusion (PBF-LB/M) and final porosity in AlSi10Mg, samples were processed following a space-filling experimental design in the present study. A total of 144 samples were fabricated considering layer thicknesses of 30 µm, 45 µm, 60 µm, and 90 µm. Afterwards, porosity was assessed using image analysis and ...
Aufsatz
On the influence of ϰ-carbides on the low-cycle fatigue behavior of high-Mn light-weight steels
(2021)
High-manganese light-weight steels offer a great potential for structural purposes in the mobility sector due to their reduced density combined with outstanding mechanical properties. As many of the envisaged applications of these materials will suffer from cyclic loading during their service life, the fundamentals of their fatigue behavior must be studied extensively. In the present work, the low-cycle fatigue (LCF) properties of an austenitic Fe-29.8Mn-7.65Al-1.11C light-weight steel were investigated. Two ...
Aufsatz
On the structural integrity of Fe-36Ni Invar alloy processed by selective laser melting
(2020)
Specimens made from pre-alloyed Invar (Fe-36Ni) powder were fabricated by selective laser melting and stress-relief heat treated afterwards. A relative density of the fabricated parts of 99.6 % was determined by computed tomography. The microstructure and mechanical behavior under monotonic and particularly cyclic loading at ambient temperature were investigated. Results reveal a bimodal microstructure containing columnar and equiaxed grains with an average grain size of 75 μm and pronounced texture 〈001〉 || BD. The ...
Aufsatz
Pathways toward the Use of Non-Destructive Micromagnetic Analysis for Porosity Assessment and Process Parameter Optimization in Additive Manufacturing of 42CrMo4 (AISI 4140)
(2024-02-20)
Laser-based powder bed fusion of metals (PBF-LB/M) is a widely applied additive manufacturing technique. Thus, PBF-LB/M represents a potential candidate for the processing of quenched and tempered (Q&T) steels such as 42CrMo4 (AISI 4140), as these steels are often considered as the material of choice for complex components, e.g., in the toolmaking industry. However, due to the presence of process-induced defects, achieving a high quality of the resulting parts remains challenging in PBF-LB/M. Therefore, an extensive ...
Aufsatz
Bend Straightening of a Carbonitrided Gear Shaft – Consequences on Residual Stresses and Retained Austenite near the Surface
(2017-06-20)
Carbonitriding of shafts in drive technology is strongly connected with distortion. Bend straightening is an important process step in order to eliminate distortion without removing the hardened surface layer. As shown in several investigations, even for simple part geometries, bending induced stresses and plastic deformations have a strong impact not only on the residual stress state but also on the microstructure after straightening. As gear shafts become increasingly filigree and complex in their geometry, the ...