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Novel Class of Rhenium Borides Based on Hexagonal Boron Networks Interconnected by Short B₂ Dumbbells
(2022-09-06)
Transition metal borides are known due to their attractive mechanical, electronic, refractive, and other properties. A new class of rhenium borides was identified by synchrotron single-crystal X-ray diffraction experiments in laser-heated diamond anvil cells between 26 and 75 GPa. Recoverable to ambient conditions, compounds rhenium triboride (ReB₃) and rhenium tetraboride (ReB₄) consist of close-packed single layers of rhenium atoms alternating with boron networks built from puckered hexagonal layers, which link ...
Aufsatz
A new method for microscale cyclic crack growth characterization from notched microcantilevers and application to single crystalline tungsten and a metallic glass
(2022-06-22)
The lifetime of most metals is limited by cyclic loads, ending in fatigue failure. The progressive growth of cracks ends up in catastrophic failure. An advanced method is presented for the determination of cyclic crack growth on the microscale using a nanoindenter, which allows the characterization of > 10,000 loading cycles. It uses focused ion beam fabricated notched microcantilevers. The method has been validated by cyclic bending metallic glass and tungsten microcantilevers. The experiments reveal a stable crack ...
Aufsatz
Effect of Cell Morphology on Flexural Behavior of Injection-Molded Microcellular Polycarbonate
(2022-05-19)
The quantitative study of the structure and properties relationship in cellular materials is mostly limited to cell diameter, cell density, skin layer thickness, and cell size distribution. In addition, the investigation of the morphology is generally carried out in two dimensions. Therefore, the
interrelation between morphological properties and mechanical characteristics of the foam structure has remained in an uncertain state. In this study, during the physical foaming process, a foam morphology is locally created ...
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Mechanics of colloidal supraparticles under compression
(2021-10-13)
Colloidal supraparticles are finite, spherical assemblies of many primary particles. To take advantage of their emergent functionalities, such supraparticles must retain their structural integrity. Here, we investigate their size-dependent mechanical properties via nanoindentation. We find that the deformation resistance inversely scales with the primary particle diameter, while the work of deformation is dependent on the supraparticle diameter. We adopt the Griffith theory to such particulate systems to provide a ...
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On data-driven nonlinear uncertainty modeling: Methods and application for control-oriented surface condition prediction in hard turning
(2020-10-16)
In this article, two data-driven modeling approaches are investigated, which allow an explicit modeling of uncertainty. For this purpose, parametric Takagi-Sugeno multi-models with bounded-error parameter estimation and nonparametric Gaussian process regression are applied and compared. These models can for instance be used for robust model-based control design. As an application, the prediction of residual stresses during hard turning depending on the machining parameters and the initial hardness is considered.
Aufsatz
Hydrogen absorption of ultra-high strength aluminum-silicon coated 22MnB5 steels
(2022-12-30)
The hot forming process allows to produce safety-relevant structural components in the automotive industry with strengths of 1500 MPa and higher. Generally, high strengths make material sensitive to hydrogen embrittlement. The heat treatment in the hot forming process chain is a potential source of diffusible hydrogen for hot-dipped aluminum-silicon coated boron-manganese steels. In the present work, the influence of different process gases and furnace dwell times during the heat treatment was investigated. Humidified ...
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Constant Temperature Approach for the Assessment of Injection Molding Parameter Influence on the Fatigue Behavior of Short Glass Fiber Reinforced Polyamide 6
(2021-05-13)
Short glass fiber reinforced plastics (SGFRP) offer superior mechanical properties compared to polymers, while still also enabling almost unlimited geometric variations of components at large-scale production. PA6-GF30 represents one of the most used SGFRP for series components, but the impact of injection molding process parameters on the fatigue properties is still insufficiently investigated. In this study, various injection molding parameter configurations were investigated on PA6-GF30. To take the significant ...
Aufsatz
Thermal Properties of Plasticized Cellulose Acetate and Its β-Relaxation Phenomenon
(2021-04-21)
Cellulose acetate (CA), an organic ester, is a biobased polymer which exhibits good mechanical properties (e.g., high Young’s modulus and tensile strength). In recent decades, there has been significant work done to verify the thermal and thermomechanical behaviors of raw and plasticized cellulose acetate. In this study, the thermomechanical properties of plasticized cellulose acetate—especially its β-relaxation and activation energy—were investigated. The general thermal behavior was analyzed and compared with ...
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Microstructural and mechanical properties of AlSi10Mg: Hybrid welding of additively manufactured and cast parts
(2022-12-07)
Welding and joining of hybrid components consisting of additively manufactured (AM) parts and conventionally processed parts offer new opportunities in structural design. In the present study, AlSi10Mg specimens were fabricated using two different manufacturing processes, i.e., laser-based powder-bed fusion of metals (PBF-LB/M) and casting, and welded by means of friction stir welding (FSW). Material strength of dissimilar welded joints was found to be governed by the as-cast material, which is characterized by a ...
Aufsatz
Additive Manufacturing of Binary Ni–Ti Shape Memory Alloys Using Electron Beam Powder Bed Fusion: Functional Reversibility Through Minor Alloy Modification and Carbide Formation
(2022-11-30)
Shape memory alloys (SMAs), such as Ni–Ti, are promising candidates for actuation and damping applications. Although processing of Ni–Ti bulk materials is challenging, well-established processing routes (i.e. casting, forging, wire drawing, laser cutting) enabled application in several niche applications, e.g. in the medical sector. Additive manufacturing, also referred to as 4D-printing in this case, is known to be highly interesting for the fabrication of SMAs in order to produce near-net-shaped actuators and ...