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Effects of aging on the stress-induced martensitic transformation and cyclic superelastic properties in Co-Ni-Ga shape memory alloy single crystals under compression
(2022)
Co-Ni-Ga shape memory alloys attracted scientific attention as promising candidate materials for damping applications at elevated temperatures, owing to excellent superelastic properties featuring a fully reversible stress-strain response up to temperatures as high as 500 °C. In the present work, the effect of aging treatments conducted in a wide range of aging temperatures and times, i.e. at 300–400 °C for 0.25–8.5 h, was investigated. It is shown that critical features of the martensitic transformation are strongly ...
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Additive manufacturing of Co-Ni-Ga high-temperature shape memory alloy - Processability 3 and phase transformation behavior
(2019)
Co-Ni-Ga high-temperature shape memory alloy is additively processed by selective laser melting for the first time. Reversiblemartensitic transformation of the as-built material is proven by differential scanning calorimetry. Microstructural analysis reveals a columnar-grained microstructure due to epitaxial solidification. Columnar-grained microstructures are characterized by a very low degree of constraints being beneficial for superior functional performance in numerous shape memory alloys. However, process-induced ...
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Investigations on Tightness of Polymer-Metal Hybrids in Environments with Thermal, Media, and Mechanical Loads
(2017-07-31)
With polymer-metal hybrids becoming more commonly used as structural components it was investigated how they perform in complex environments with combined thermal, media, and mechanical loads. Special attention was put on media tightness under said loads. This paper sums up the activities of the polymer technology research group of the University of Kassel on hybrids produced by overmolding metal inserts. Investigations concerning joint strength and influence of (cyclic) temperature loads and chemical corrosion on ...
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Mechanical Properties of Polydimethylsiloxane as a Function of the Amount and Type of Crosslinking Agent
(2017-06-13)
In this investigation, a high-consistency rubber (HCR) was mixed with five different, typically used crosslinking agents that are based on organic peroxide. Furthermore, the amount of crosslinking agent was varied in order to quantify the effect on the mechanical properties. All materials were processed in a hot pressing process, and, subsequently, post-cured. The properties were characterized by the measurement of the swelling ratio, shore A-hardness, rebound resilience and tensile test. We successfully proved that ...
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Microstructure of an additively manufactured Ti-Ta-Al alloy using novel pre-alloyed powder feedstock material
(2023-05-01)
Binary Ti-Ta and ternary Ti-Ta-Al alloys attracted considerable attention as new potential biomaterials and/or high-temperature shape memory alloys. However, conventional forming and manufacturing technologies of refractory based titanium alloys are difficult and cost-intensive, especially when complex shapes are required. Recently, additive manufacturing (AM) emerged as a suitable alternative and several studies exploited elemental powder mixing approaches to obtain a desired alloy and subsequently use it for complex ...
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Pathways towards grain boundary engineering for improved structural performance in polycrystalline Co-Ni-Ga shape memory alloys
(2018)
Co-Ni-Ga high-temperature shape memory alloys attracted a lot of scientific attention due to their superior functional material properties in recent years. In the single crystalline state Co-Ni-Ga HT-SMAs feature a good pseudoelastic response up to 500°C. However, in the polycrystalline condition Co-Ni-Ga suffers significant grain constraints and premature fracture at grain boundaries. In this regard, crystallographic orientation of the grain being involved as well as morphology and geometrical orientation of the ...
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Influence of ethylene oxide and gamma irradiation sterilization processes on the degradation behaviour of poly(lactic acid) (PLA) in the course of artificially accelerated aging
(2024-02-10)
To promote the application of bio-based materials in the field of medical technology, it is essential to conduct additional research, focusing on their long-term performance after sterilization. For this purpose, the study examines the aging behaviour of three poly(lactic-acid) (PLA) materials, sterilized with either ethylene oxide or gamma irradiation, over a two years aging period, in accordance with ASTM F1980-21. During these investigations, a direct correlation between moisture absorption and degradation progression ...
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Characterization of polyamide 6.10 composites incorporated with microcrystalline cellulose fiber: Effects of fiber loading and impact modifier
(2018-08-14)
Microcrystalline cellulose (MCC) fiber‐reinforced polyamide 6.10 (PA) composites were prepared in the presence of an impact modifier (IM), exxelor VA1803 (VA), by melt compounding process. Fiber loading was considered from 20 to 30 wt.%, whereas IM was varied from 2.0 to 5.0 wt.%. Composites were characterized by tensile test, impact test, dynamic thermal mechanical analysis (DTMA), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and X‐ray diffraction (XRD). Composites’ fractured surfaces ...
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Fabrication and characterization of ethylene–octene copolymer composites with ionic liquid functionalized carbon nanotubes
(2017-10-16)
Modification of multi-walled carbon nanotubes (MWCNTs) by means of imidazolium ionic liquid (IL) was performed. Structural characterization of funtionalized nanofillers (IL-f-MWCNTs) was made by means of Raman spectroscopy and transmission electron microscopy. MWCNTs and IL-f-MWCNTs were introduced within ethylene octane copolymer (EOC) with octene co-monomer content of 17% by using the masterbatch approach. The efficiency of the carbonaceous nanofiller distribution within the polymer matrix was characterized by means ...
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Effect of nanometric γ´-particles on the stress-induced martensitic transformation in ⟨001⟩-oriented Co49Ni21Ga30 shape memory alloy single crystals
(2019)
The effect of finely dispersed particles on the functional properties and morphology of thermally induced martensite in Co-Ni-Ga shape memory alloys has been already reported in literature, however, still important aspects are not fully understood. The current study focuses on the stress-induced martensitic transformation of solution-annealed, i.e. precipitate-free, and aged 〈001〉-oriented single crystals. In situ optical microscopy and neutron diffraction experiments show a significant influence of γ′-particles on ...