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Structural reorientation and compaction of porous MoS₂ coatings during wear testing
(2022-04-02)
Industrial upscaling frequently results in a different coating microstructure than the laboratory prototypes presented in the literature. Here, we investigate the wear behavior of physical vapor deposited (PVD) MoS2 coatings: A dense, nanocrystalline MoS2 coating, and a porous, prismatic-textured MoS2 coating. Transmission electron microscopy (TEM) investigations before and after wear testing evidence a crystallographic reorientation towards a basal texture in both samples. A basal texture is usually desirable due ...
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Microstructural Constituents and Mechanical Properties of Low-Density Fe-Cr-Ni-Mn-Al-C Stainless Steels
(2022-07-23)
Metallic material concepts associated with the sustainable and efficient use of resources are currently the subject of intensive research. Al addition to steel offers advantages in view of lightweight, durability, and efficient use of high-Fe scrap from the Al industry. In the present work, Al was added to Fe-12Cr-(9,12)Ni-3Mn-0.3C-xAl (x = 0.1–6) (wt.%) stainless steels to assess its influence on microstructure and mechanical properties. According to density measurements based on Archimedes’ principle, densities ...
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Microcantilever Fracture Tests of α-Cr Containing NiAl Bond Coats
(2022-01-08)
MCrAlY bond coats are widely used as oxidation-resistant coatings on superalloys. The major phase is the thermally stable intermetallic β-NiAl phase. The addition of Cr increases the oxidation and corrosion resistance but leads to the formation of α-Cr precipitates. Both phases are brittle and limit the fracture toughness of these coatings. To study the influence of thermal exposure and the resulting changing chemical composition on the fracture properties, the fracture toughness of both phases is measured by notched ...
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Microstructural and Mechanical Properties of AISI 4140 Steel Processed by Electron Beam Powder Bed Fusion Analyzed Using Miniature Samples
(ASTM International, 2022-02-26)
The present study reports on the identification of an adequate process window for electron beam powder bed fusion (E-PBF) of AISI 4140 steel. For characterization, only miniature samples were used. It is clearly revealed that, for comparison and evaluation of different conditions, the use of such small samples is absolutely sufficient, even under fatigue loading. The initial E-PBF as-built condition is compared with conventionally heat-treated conditions (i.e., normalized as well as quenched and tempered). Based on ...
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Investigation of processing windows in additive manufacturing of AlSi10Mg for faster production utilizing data-driven modeling
(2022-04-29)
To reduce production time and decrease production cost, the increase of layer thickness is an adequate option in powder bed fusion. In order to determine the relationships between process parameters in laser powder bed fusion (PBF-LB/M) and final porosity in AlSi10Mg, samples were processed following a space-filling experimental design in the present study. A total of 144 samples were fabricated considering layer thicknesses of 30 µm, 45 µm, 60 µm, and 90 µm. Afterwards, porosity was assessed using image analysis and ...
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Microstructural and mechanical properties of AlSi10Mg: Hybrid welding of additively manufactured and cast parts
(2022-12-07)
Welding and joining of hybrid components consisting of additively manufactured (AM) parts and conventionally processed parts offer new opportunities in structural design. In the present study, AlSi10Mg specimens were fabricated using two different manufacturing processes, i.e., laser-based powder-bed fusion of metals (PBF-LB/M) and casting, and welded by means of friction stir welding (FSW). Material strength of dissimilar welded joints was found to be governed by the as-cast material, which is characterized by a ...
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Additive Manufacturing of Binary Ni–Ti Shape Memory Alloys Using Electron Beam Powder Bed Fusion: Functional Reversibility Through Minor Alloy Modification and Carbide Formation
(2022-11-30)
Shape memory alloys (SMAs), such as Ni–Ti, are promising candidates for actuation and damping applications. Although processing of Ni–Ti bulk materials is challenging, well-established processing routes (i.e. casting, forging, wire drawing, laser cutting) enabled application in several niche applications, e.g. in the medical sector. Additive manufacturing, also referred to as 4D-printing in this case, is known to be highly interesting for the fabrication of SMAs in order to produce near-net-shaped actuators and ...
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Electrochemical polarization behavior and superelastic properties of a Fe–Mn–Al–Ni–Cr shape memory alloy
(2022-10-22)
The present study investigates the corrosion behavior of a Fe–Mn–Al–Ni–Cr shape memory alloy in a 5.0 wt% NaCl solution in combination with the functional properties. In a single crystalline condition, the investigated alloy shows a superior superelastic response with a maximum recovery strain of 5.2%. Furthermore, the results of the potentiodynamic polarization and impedance spectroscopy show that the addition of chromium generally improves corrosion resistance by increasing the resistance to localized corrosion. ...
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A Novel Thermo-Mechanical Processing Route Exploiting Abnormal Grain Growth in Heusler-Type Co–Ni–Ga Shape Memory Alloys
(2022-10-04)
Heusler-type Co–Ni–Ga shape memory alloys attracted significant scientific attention owing to excellent superelasticity in single-crystalline state. However, due to pronounced anisotropy, polycrystalline Co–Ni–Ga suffers from transformation-induced constraints at grain boundaries and, thus, premature failure upon thermo-mechanical loading. The present study reports on a novel thermo-mechanical processing route. Hot rolling followed by solution-annealing promotes abnormal grain growth, eventually leading to high-performance ...
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Cooling rate as a process parameter in advanced roll forming to tailor microstructure,mechanical and corrosion properties of EN AW 7075 tubes
(2022-12-14)
The effects of solution heat treatment parameters and quench media as a processing tool for tailoring microstructure, mechanical and corrosion properties in roll forming of EN AW 7075 alloy were studied. The highest yield stress and ultimate tensile strength were obtained for the specimens quenched in water, while the air-cooled specimens exhibited inferior mechanical properties. Microstructural analysis of specimens showed that except water-quenched specimens, the parts cooled/quenched in oil, in direct contact with ...