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Fabrication and characterization of ethylene–octene copolymer composites with ionic liquid functionalized carbon nanotubes
(2017-10-16)
Modification of multi-walled carbon nanotubes (MWCNTs) by means of imidazolium ionic liquid (IL) was performed. Structural characterization of funtionalized nanofillers (IL-f-MWCNTs) was made by means of Raman spectroscopy and transmission electron microscopy. MWCNTs and IL-f-MWCNTs were introduced within ethylene octane copolymer (EOC) with octene co-monomer content of 17% by using the masterbatch approach. The efficiency of the carbonaceous nanofiller distribution within the polymer matrix was characterized by means ...
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Crack path predictions in fiber reinforced composites
(2017-09-06)
Composite materials exhibit beneficial features compared to conventional engineering material, e.g. a comparable strength and a reduced weight at the same time. To fully exploit these beneficial properties within technical structures, fracture mechanical concepts must be taken into account. The global fracture behavior in composite materials is related to the local delamination at interfaces between matrix and inclusion as well as the local fracture behaviors of the constituents. Because of their structure, the global ...
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Comparative investigation of two-dimensional imaging methods and X-ray tomography in the characterization of microstructure
(2017-10-02)
The microstructural features of three different materials have been quantified by means of 2D image analysis and X-ray micro-computer tomography (CT) and the results were compared to determine the reliability of the 2D analysis in the material characterization. The 3D quantification of shrinkage pores and Fe-rich inclusions of an Al-Si-Cu alloy by X-ray tomography was compared with the statistical analysis of the 2D metallographic pictures and a significant difference in the results was found due to the complex ...
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Electron beam welding of Fe–Mn–Al–Ni shape memory alloy: Microstructure evolution and shape memory response
(2017-07-03)
The present study reports on the impact of abnormal grain growth (AGG) on the microstructural evolution following electron beam (EB) welding of Fe–Mn–Al–Ni shape memory alloy (SMA). Polycrystalline sheet-like material was EB-welded and a cyclic heat treatment, studied in previous work, was conducted for inducing AGG and a bamboo-like microstructure, respectively. Optical and electron microscopy were carried out to characterize the prevailing microstructure upon cyclic heat treatment. For characterization of the ...
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Time-of-Flight Three Dimensional Neutron Diffraction in Transmission Mode for Mapping Crystal Grain Structures
(2017-08-25)
The physical properties of polycrystalline materials depend on their microstructure, which is the nano- to centimeter scale arrangement of phases and defects in their interior. Such microstructure depends on the shape, crystallographic phase and orientation, and interfacing of the grains constituting the material. This article presents a new non-destructive 3D technique to study centimeter-sized bulk samples with a spatial resolution of hundred micrometers: time-of-flight three-dimensional neutron diffraction (ToF ...
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Energy Resolved Residual Stress Analysis with Laboratory X-Ray Sources
(2017-04-17)
It is well known that existing residual stress fields play an important role for strength and lifetime of components. Consequently there is a great interest in the availability of fast, reliable and possibly nondestructive methods for their determination. In this context, X-ray diffraction methods play an important role in technical practice as well as in scientific research. They are based on the determination of lattice strains from which residual stresses are determined applying Hooke's law with appropriate elastic ...
Aufsatz
Bend Straightening of a Carbonitrided Gear Shaft – Consequences on Residual Stresses and Retained Austenite near the Surface
(2017-06-20)
Carbonitriding of shafts in drive technology is strongly connected with distortion. Bend straightening is an important process step in order to eliminate distortion without removing the hardened surface layer. As shown in several investigations, even for simple part geometries, bending induced stresses and plastic deformations have a strong impact not only on the residual stress state but also on the microstructure after straightening. As gear shafts become increasingly filigree and complex in their geometry, the ...