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Aufsatz
Martensite aging in ⟨001⟩ oriented Co₄₉ Ni₂₁ Ga₃₀ single crystals in tension
(2018-03-22)
Co–Ni–Ga high-temperature shape memory alloys (HT-SMAs) are well-known candidate materials for damping applications at elevated temperatures. Recent studies showed that upon heat treatment in stress-induced martensite under compressive loads transformation temperatures can be increased significantly, qualifying Co–Ni–Ga for HT-actuation. The increase in transformation temperatures is related to a change in chemical order recently validated via neutron diffraction experiments. Since SMAs show distinct tension–compression ...
Aufsatz
Electron beam welding of Fe–Mn–Al–Ni shape memory alloy: Microstructure evolution and shape memory response
(2017-07-03)
The present study reports on the impact of abnormal grain growth (AGG) on the microstructural evolution following electron beam (EB) welding of Fe–Mn–Al–Ni shape memory alloy (SMA). Polycrystalline sheet-like material was EB-welded and a cyclic heat treatment, studied in previous work, was conducted for inducing AGG and a bamboo-like microstructure, respectively. Optical and electron microscopy were carried out to characterize the prevailing microstructure upon cyclic heat treatment. For characterization of the ...
Aufsatz
Processing effects on tensile superelastic behaviour of Fe43.5Mn34Al15 ± XNi7.5∓X shape memory alloys
(2019)
Fe₄₃.₅Mn₃₄Al₁₅Ni₇.₅ was introduced in the current decade as a new superelastic alloy with great applicative potential due to: (i) superelastic behaviour over a thermal range of 200°C and (ii) recoverable strains up to 9.7 %. One of the key factors in enhancing the superelastic response of several shape memory alloys (SMAs) is the formation of an oligocrystalline structure, i.e. without triple junctions between grains, which is the result of an abnormal grain growth (AGG) process that can be induced by cyclic heat ...
Aufsatz
Design of novel materials for additive manufacturing - Isotropic microstructure and high defect tolerance
(2018-01-22)
Electron Beam Melting (EBM) is a powder-bed additive manufacturing technology enabling the production of complex metallic parts with generally good mechanical properties. However, the performance of powder-bed based additively manufactured materials is governed by multiple factors that are difficult to control. Alloys that solidify in cubic crystal structures are usually affected by strong anisotropy due to the formation of columnar grains of preferred orientation. Moreover, processing induced defects and porosity ...
Aufsatz
Shape memory effect and superelasticity in high-strength FeNiCoAlTi single crystals hardened by nanoparticles
(2019-11-19)
For [001]-oriented single crystals of Fe-28Ni-17Co-11.5Al-2.5Ti (at %) alloy in tension, it was shown that particles of the γ’-phase with a size of 4–6 nm lead to the appearance of superelasticity, with a strain of εSE=4.5% and a shape memory effect of εSME=5.9%. Increasing the particle size to 10–12 nm reduces εSE to 3.6% and εSME to 3.5%. The paper discusses the causes of the influence of particle size on the reversible strain.
Aufsatz
On the Effect of Quenching on Postweld Heat Treatment of Friction-Stir-Welded Aluminum 7075 Alloy
(2019)
This work focuses on the effect of postweld heat treatment (PWHT) on the mechanical properties and microstructural evolution of aluminum 7075 alloy processed via friction stir welding (FSW). FSW is known to be capable of grain refinement in the nugget zone (NZ). Two different quench media (water and air) were employed for PWHT. Regardless of the quench media, the PWHT led to the occurrence of grain growth in the NZ of the FSWed aluminum 7075 alloy. Abnormal grain growth occurred in the water quenched specimen. It is ...
Aufsatz
Cyclic Deformation Response of Ultra-fine Grained Titanium at Elevated Temperatures
(2019)
This study focuses on the high-temperature cyclic deformation response (CDR) of ultra-fine grained (UFG) titanium of commercial purity (grade 4) processed via equal channel angular extrusion as a severe plastic deformation method. Low-cycle fatigue experiments were conducted at elevated temperatures up to 600 °C and at strain amplitudes ranging from 0.2% to 0.6%. Besides temperature and strain amplitude, the influence of two processing routes (8BC and 8E) on the fatigue characteristics of UFG Ti was examined. It is ...
Aufsatz
Effect of grain size on the very high cycle fatigue behavior and notch sensitivity of titanium
(2019)
The very high-cycle fatigue performances of coarse-grained and ultrafine-grained titanium samples with different geometries at ambient temperature and various stress amplitudes were investigated. Severe plastic deformation improves monotonic strength of titanium at the cost of a loss in ductility. Ultrafine-grained titanium demonstrates a superior fatigue performance compared to that of coarse-grained counterparts in the high-cycle fatigue regime, however, suffers notch sensitivity. Furthermore, in the very high-cycle ...
Aufsatz
Effect of nanometric γ´-particles on the stress-induced martensitic transformation in ⟨001⟩-oriented Co49Ni21Ga30 shape memory alloy single crystals
(2019)
The effect of finely dispersed particles on the functional properties and morphology of thermally induced martensite in Co-Ni-Ga shape memory alloys has been already reported in literature, however, still important aspects are not fully understood. The current study focuses on the stress-induced martensitic transformation of solution-annealed, i.e. precipitate-free, and aged 〈001〉-oriented single crystals. In situ optical microscopy and neutron diffraction experiments show a significant influence of γ′-particles on ...
Aufsatz
Promoting abnormal grain growth in Fe-based shape memory alloys through compositional adjustments
(2019-05-28)
Iron-based shape memory alloys are promising candidates for large-scale structural applications due to their cost efficiency and the possibility of using conventional processing routes from the steel industry. However, recently developed alloy systems like Fe–Mn–Al–Ni suffer from low recoverability if the grains do not completely cover the sample cross-section. To overcome this issue, here we show that small amounts of titanium added to Fe–Mn–Al–Ni significantly enhance abnormal grain growth due to a considerable ...