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Structural reorientation and compaction of porous MoS₂ coatings during wear testing
(2022-04-02)
Industrial upscaling frequently results in a different coating microstructure than the laboratory prototypes presented in the literature. Here, we investigate the wear behavior of physical vapor deposited (PVD) MoS2 coatings: A dense, nanocrystalline MoS2 coating, and a porous, prismatic-textured MoS2 coating. Transmission electron microscopy (TEM) investigations before and after wear testing evidence a crystallographic reorientation towards a basal texture in both samples. A basal texture is usually desirable due ...
Aufsatz
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Tribological Performance of Additively Manufactured AISI H13 Steel in Different Surface Conditions
(2021-02-16)
Additive manufacturing of metallic tribological components offers unprecedented degrees of freedom, but the surface roughness of most as-printed surfaces impedes the direct applicability of such structures, and postprocessing is necessary. Here, the tribological performance of AISI H13 steel samples was studied. These were additively manufactured through laser powder bed fusion (L-PBF), also referred to as selective laser melting (SLM). Samples were tested in four different surface conditions: as-printed, polished, ...
Aufsatz
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Additive Manufacturing of Compositionally-Graded AISI 316L to CoCrMo Structures by Directed Energy Deposition
(2021-08-30)
In the present study, compositionally-graded structures of AISI 316L and CoCrMo alloy are manufactured by powder-based laser-beam directed energy deposition (DED-LB). Through a process-integrated adjustment of powder flow, in situ alloying of the two materials becomes feasible. Thus, a sharp and a smooth transition with a mixture of both alloys can be realized. In order to investigate the phase formation during in situ alloying, a simulation approach considering equilibrium calculations is employed. The findings ...
Aufsatz
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Overmoulding of Additively Manufactured Titanium Inserts Using Polyoxymethylene (POM)—Evaluation of Bond Quality as a Function of Process Parameters
(2021-06-15)
Due to their process-induced porous surfaces, additively manufactured structures are not optimized for applications in which friction is a key factor. To improve the frictional properties of additively manufactured titanium inserts of various thicknesses, two tribologically optimized POM materials, which differ in terms of filler composition and contents, were used to overmould the inserts. The titanium inserts were manufactured in two different building directions, resulting in a variation in surface roughness. The ...
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Microstructural Constituents and Mechanical Properties of Low-Density Fe-Cr-Ni-Mn-Al-C Stainless Steels
(2022-07-23)
Metallic material concepts associated with the sustainable and efficient use of resources are currently the subject of intensive research. Al addition to steel offers advantages in view of lightweight, durability, and efficient use of high-Fe scrap from the Al industry. In the present work, Al was added to Fe-12Cr-(9,12)Ni-3Mn-0.3C-xAl (x = 0.1–6) (wt.%) stainless steels to assess its influence on microstructure and mechanical properties. According to density measurements based on Archimedes’ principle, densities ...
Aufsatz
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Microcantilever Fracture Tests of α-Cr Containing NiAl Bond Coats
(2022-01-08)
MCrAlY bond coats are widely used as oxidation-resistant coatings on superalloys. The major phase is the thermally stable intermetallic β-NiAl phase. The addition of Cr increases the oxidation and corrosion resistance but leads to the formation of α-Cr precipitates. Both phases are brittle and limit the fracture toughness of these coatings. To study the influence of thermal exposure and the resulting changing chemical composition on the fracture properties, the fracture toughness of both phases is measured by notched ...
Aufsatz
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Determination and Validation of Residual Stresses in CFRP/Metal Hybrid Components Using the Incremental Hole Drilling Method
(2020-09-21)
Lightweight materials contribute to an efficient decrease in fuel consumption in the automotive and aircraft industries. Hybrid components made of metal and carbon fiber-reinforced plastics (CFRP) have a high potential in lightweight applications due to their high strength-to-weight ratio. For cost-effective processing of hybrid materials, advanced manufacturing processes such as the prepreg-press-technology have been developed, in which the bonding between a metallic component and a fiber compound is exclusively ...
Dissertation
Oberflächennahe Schädigung von Superlegierungen unter Hochtemperatur
(2020-02)
In der vorliegenden Arbeit wird die Alterung von Nickelbasislegierungen in Oberflächennähe betrachtet. Dabei wird der Einfluss von Temperatur und Zeit in Zusammenhang mit der Oberflächenrauheit, Deformation und der Konzentration von Natriumsulfat an der Probenoberfläche untersucht. Zur Quantifizierung der Schädigung kommen rasterelektronenmikroskopische Methoden wie EBSD und EDX zum Einsatz.
Es wird gezeigt, dass die analysierten Verarmungs- und Vergröberungsprozesse der Gamma'-Ausscheidungen eine deutliche ...
Konferenzveröffentlichung
Microstructural and Mechanical Properties of AISI 4140 Steel Processed by Electron Beam Powder Bed Fusion Analyzed Using Miniature Samples
(ASTM International, 2022-02-26)
The present study reports on the identification of an adequate process window for electron beam powder bed fusion (E-PBF) of AISI 4140 steel. For characterization, only miniature samples were used. It is clearly revealed that, for comparison and evaluation of different conditions, the use of such small samples is absolutely sufficient, even under fatigue loading. The initial E-PBF as-built condition is compared with conventionally heat-treated conditions (i.e., normalized as well as quenched and tempered). Based on ...
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Investigation of processing windows in additive manufacturing of AlSi10Mg for faster production utilizing data-driven modeling
(2022-04-29)
To reduce production time and decrease production cost, the increase of layer thickness is an adequate option in powder bed fusion. In order to determine the relationships between process parameters in laser powder bed fusion (PBF-LB/M) and final porosity in AlSi10Mg, samples were processed following a space-filling experimental design in the present study. A total of 144 samples were fabricated considering layer thicknesses of 30 µm, 45 µm, 60 µm, and 90 µm. Afterwards, porosity was assessed using image analysis and ...