SEM-DIC characterization of the damage mechanism of an AlSi10Fe0.7 casting alloy on the microstructure scale
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In: Materials Characterization Volume 218, Part 1 / (2024-10-20) , S. ; eissn:1873-4189
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Various brittle phases are present in commercial cast aluminum alloys, which strongly influence their mechanical behavior. Among these, silicon precipitates are nearly omnipresent, as Si is a common alloying element. In secondary alloys, usually Fe-containing phases cannot be avoided, and they tend to degrade the mechanical properties. The interaction between the silicon phase and the failure-critical intermetallic phase in the Al-Si-Fe phase system (β-AI₅FeSi) is studied in this paper in high resolution. A model alloy AlSi10Fe0.7 was defined, which is composed of a large grain Al-matrix, Si-precipitates and the plate-like β-AI₅FeSi phase. The goal of the study was to identify “hot spots” in the microstructure from which cracks may initiate under mechanical loading. The main tool was a deformation analysis via digital image correlation in the SEM (SEM-DIC). This allows the identification and tracking of developing strain localizations at different potential crack initiation sites with a high resolution as well as capturing an overview over the whole specimen. An adapted frame averaging script minimized measurement errors induced by drift. The SEM-DIC results show that the deformation field is governed by the elastic incompatibility of the microstructural constituents. Crack initiation occurs because of the detachment of the Si + β-AI₅FeSi phase boundary. Cracks then cross the phase boundary and propagate along twin boundaries in the β-AI₅FeSi phase. Final failure is caused by linking fractured brittle plate-like particles.
@article{doi:10.17170/kobra-2024112010691, author ={Ickler, Tim and Jüngst, Daniel and Meckbach, Heiko and Zeismann, Frank and Brückner-Foit, Angelika and Fehlbier, Martin}, title ={SEM-DIC characterization of the damage mechanism of an AlSi10Fe0.7 casting alloy on the microstructure scale}, keywords ={600 and Bildkorrelation and Elektronenmikroskopie and Aluminiumlegierung and Gusslegierung and Rissbildung and Mechanische Eigenschaft}, copyright ={http://creativecommons.org/licenses/by/4.0/}, language ={en}, journal ={Materials Characterization}, year ={2024-10-20} }