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Aufsatz
Micromechanical Modeling of AlSi10Mg Processed by Laser-Based Additive Manufacturing: From as-Built to Heat-Treated Microstructures
(2022-08-13)
The unique microstructure of the alloy AlSi10Mg produced by the laser-based powder bed fusion of metals (PBF-LB/M) provides high-strength and high-strain-hardening capabilities of the material. The microstructure and mechanical properties of 3D-printed, i.e., additively manufactured, AlSi10Mg are significantly altered by post-building heat-treatment processes applied in order to tailor the final properties of the parts. Using an accurate computational model to predict and improve the mechanical performance of 3D-printed ...
Aufsatz
Linking through-thickness cracks in metallic thin films to in-situ electrical resistance peak broadening
(2022-01-29)
Measurements of electrical resistance have been used extensively as a failure criterion in cyclically loaded conductive films. However, not much research has been performed on extracting additional information contained within such resistance data sets. This study shows that an increase in peak width evidences a transition from cracks bridging to through-thickness crack formation. A Au/Cr bilayer system on a polyimide substrate is used for data generation but the method is applicable to any material system where both ...
Aufsatz
Additive Manufacturing of 3D Luminescent ZrO2:Eu3+ Architectures
(2022-04-27)
Implementation of more refined structures at the nano to microscale is expected to advance applications in optics and photonics. This work presents the additive manufacturing of 3D luminescent microarchitectures emitting light in the visible range. A tailor-made organo-metallic resin suitable for two-photon lithography is developed, which upon thermal treatment in an oxygen-rich atmosphere allows the creation of silicon-free tetragonal (t-) and monoclinic (m-) ZrO₂. The approach is unique because the tailor-made ...
Aufsatz
Structural reorientation and compaction of porous MoS₂ coatings during wear testing
(2022-04-02)
Industrial upscaling frequently results in a different coating microstructure than the laboratory prototypes presented in the literature. Here, we investigate the wear behavior of physical vapor deposited (PVD) MoS2 coatings: A dense, nanocrystalline MoS2 coating, and a porous, prismatic-textured MoS2 coating. Transmission electron microscopy (TEM) investigations before and after wear testing evidence a crystallographic reorientation towards a basal texture in both samples. A basal texture is usually desirable due ...
Aufsatz
Microstructural Constituents and Mechanical Properties of Low-Density Fe-Cr-Ni-Mn-Al-C Stainless Steels
(2022-07-23)
Metallic material concepts associated with the sustainable and efficient use of resources are currently the subject of intensive research. Al addition to steel offers advantages in view of lightweight, durability, and efficient use of high-Fe scrap from the Al industry. In the present work, Al was added to Fe-12Cr-(9,12)Ni-3Mn-0.3C-xAl (x = 0.1–6) (wt.%) stainless steels to assess its influence on microstructure and mechanical properties. According to density measurements based on Archimedes’ principle, densities ...
Aufsatz
Microcantilever Fracture Tests of α-Cr Containing NiAl Bond Coats
(2022-01-08)
MCrAlY bond coats are widely used as oxidation-resistant coatings on superalloys. The major phase is the thermally stable intermetallic β-NiAl phase. The addition of Cr increases the oxidation and corrosion resistance but leads to the formation of α-Cr precipitates. Both phases are brittle and limit the fracture toughness of these coatings. To study the influence of thermal exposure and the resulting changing chemical composition on the fracture properties, the fracture toughness of both phases is measured by notched ...
Konferenzveröffentlichung
Microstructural and Mechanical Properties of AISI 4140 Steel Processed by Electron Beam Powder Bed Fusion Analyzed Using Miniature Samples
(ASTM International, 2022-02-26)
The present study reports on the identification of an adequate process window for electron beam powder bed fusion (E-PBF) of AISI 4140 steel. For characterization, only miniature samples were used. It is clearly revealed that, for comparison and evaluation of different conditions, the use of such small samples is absolutely sufficient, even under fatigue loading. The initial E-PBF as-built condition is compared with conventionally heat-treated conditions (i.e., normalized as well as quenched and tempered). Based on ...
Aufsatz
Investigation of processing windows in additive manufacturing of AlSi10Mg for faster production utilizing data-driven modeling
(2022-04-29)
To reduce production time and decrease production cost, the increase of layer thickness is an adequate option in powder bed fusion. In order to determine the relationships between process parameters in laser powder bed fusion (PBF-LB/M) and final porosity in AlSi10Mg, samples were processed following a space-filling experimental design in the present study. A total of 144 samples were fabricated considering layer thicknesses of 30 µm, 45 µm, 60 µm, and 90 µm. Afterwards, porosity was assessed using image analysis and ...
Aufsatz
A comparative study using water atomized and gas atomized powder in laser powder bed fusion process – Assessment of the fatigue performance
(2022)
Gas-atomized (GA, spherical) and water-atomized (WA, spattered) commercially pure iron (cp-Fe) powders were processed using laser-based powder bed fusion, resulting in a slightly higher porosity of the WA condition. In addition to characterization of quasi-static mechanical properties, fatigue tests, which are known to be detrimentally affected by porosity, were finally considered, revealing good properties even for the WA condition. In terms of microstructure stability, the GA and WA specimens significantly differ; ...
Aufsatz
Influences on the mechanical properties of SRCs in a combined compacting and back injecting process
(2022-03-03)
In this research paper, the effects of the combined compacting and back-injection process to produce back-injected self-reinforced composites on the mechanical properties of the self-reinforced composites (SRCs) are investigated. For this purpose, the parameters barrel temperature, time of injection and holding pressure were varied for the back injection. Tensile and bending tests were carried out on the SRCs. The results show that the mechanical properties depend to a large extent on the process parameters. The ...