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Aufsatz
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Influence of Cu Addition and Microstructural Configuration on the Creep Resistance and Mechanical Properties of an Fe-Based α/α′/α″ Superalloy
(2023-01-14)
Introducing Cu nanoparticles is an effective mechanism for strengthening and toughening Fe-based materials such as ultra-high-strength steels. Herein, the effect of Cu on the mechanical properties of a novel Fe-based α/α′/α″ superalloy is studied. Compared to a Cu-free reference alloy, nanoindentation reveals an increase in hardness, which was associated with the formation of Cu nanoparticles. Both alloys show room temperature (RT) compressive plastic strain at maximum stress greater than 8%, irrespective of the ...
Aufsatz
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Additive Manufacturing of 3D Luminescent ZrO2:Eu3+ Architectures
(2022-04-27)
Implementation of more refined structures at the nano to microscale is expected to advance applications in optics and photonics. This work presents the additive manufacturing of 3D luminescent microarchitectures emitting light in the visible range. A tailor-made organo-metallic resin suitable for two-photon lithography is developed, which upon thermal treatment in an oxygen-rich atmosphere allows the creation of silicon-free tetragonal (t-) and monoclinic (m-) ZrO₂. The approach is unique because the tailor-made ...
Aufsatz
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Structural reorientation and compaction of porous MoS₂ coatings during wear testing
(2022-04-02)
Industrial upscaling frequently results in a different coating microstructure than the laboratory prototypes presented in the literature. Here, we investigate the wear behavior of physical vapor deposited (PVD) MoS2 coatings: A dense, nanocrystalline MoS2 coating, and a porous, prismatic-textured MoS2 coating. Transmission electron microscopy (TEM) investigations before and after wear testing evidence a crystallographic reorientation towards a basal texture in both samples. A basal texture is usually desirable due ...
Aufsatz
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Microcantilever Fracture Tests of α-Cr Containing NiAl Bond Coats
(2022-01-08)
MCrAlY bond coats are widely used as oxidation-resistant coatings on superalloys. The major phase is the thermally stable intermetallic β-NiAl phase. The addition of Cr increases the oxidation and corrosion resistance but leads to the formation of α-Cr precipitates. Both phases are brittle and limit the fracture toughness of these coatings. To study the influence of thermal exposure and the resulting changing chemical composition on the fracture properties, the fracture toughness of both phases is measured by notched ...
Aufsatz
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Investigation of processing windows in additive manufacturing of AlSi10Mg for faster production utilizing data-driven modeling
(2022-04-29)
To reduce production time and decrease production cost, the increase of layer thickness is an adequate option in powder bed fusion. In order to determine the relationships between process parameters in laser powder bed fusion (PBF-LB/M) and final porosity in AlSi10Mg, samples were processed following a space-filling experimental design in the present study. A total of 144 samples were fabricated considering layer thicknesses of 30 µm, 45 µm, 60 µm, and 90 µm. Afterwards, porosity was assessed using image analysis and ...
Aufsatz
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On the influence of ϰ-carbides on the low-cycle fatigue behavior of high-Mn light-weight steels
(2021)
High-manganese light-weight steels offer a great potential for structural purposes in the mobility sector due to their reduced density combined with outstanding mechanical properties. As many of the envisaged applications of these materials will suffer from cyclic loading during their service life, the fundamentals of their fatigue behavior must be studied extensively. In the present work, the low-cycle fatigue (LCF) properties of an austenitic Fe-29.8Mn-7.65Al-1.11C light-weight steel were investigated. Two ...
Aufsatz
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On the structural integrity of Fe-36Ni Invar alloy processed by selective laser melting
(2020)
Specimens made from pre-alloyed Invar (Fe-36Ni) powder were fabricated by selective laser melting and stress-relief heat treated afterwards. A relative density of the fabricated parts of 99.6 % was determined by computed tomography. The microstructure and mechanical behavior under monotonic and particularly cyclic loading at ambient temperature were investigated. Results reveal a bimodal microstructure containing columnar and equiaxed grains with an average grain size of 75 μm and pronounced texture 〈001〉 || BD. The ...
Aufsatz
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Effect of Crystallographic Orientation and Grain Boundaries on Martensitic Transformation and Superelastic Response of Oligocrystalline Fe–Mn–Al–Ni Shape Memory Alloys
(2021-07-26)
In situ tensile tests employing digital image correlation were conducted to study the martensitic transformation of oligocrystalline Fe–Mn–Al–Ni shape memory alloys in depth. The influence of different grain orientations, i.e., near-〈001〉 and near-〈101〉, as well as the influence of different grain boundary misorientations are in focus of the present work. The results reveal that the reversibility of the martensite strongly depends on the type of martensitic evolving, i.e., twinned or detwinned. Furthermore, it is ...
Aufsatz
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On the Monotonic and Cyclic Behavior of an Al-Mg-Zn-Cu-Si Compositionally Complex Alloy
(2023-08-03)
In present work, the monotonic and cyclic properties of a novel Al-Mg-Zn-Cu-Si compositionally complex alloy (CCA) are investigated. Microstructural studies reveal that a eutectic phase and fishbone-type structures are embedded in the Al-matrix. The mechanical properties of this CCA obtained under compressive loading are found to be promising. However, low ultimate strength and brittle behavior are seen under tension. The fatigue performance of the alloy in the low-cycle fatigue (LCF) regime is poor. Microstructural ...
Aufsatz
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Liquid Silicone Rubber Foams Made with Water as Blowing Agent
(2021-08-18)
Liquid silicone rubber (LSR) is primarily used in injection molding. Foamed molded parts made of LSR are almost nonexistent because the process reliability of LSR foam injection molding is currently not given. It makes sense to have suitable foaming processes for this material as well, because the density of this elastomer is about 1.15 g cm−3. With the injection molding process presented herein for foaming LSR, density reductions of up to 40% can be achieved. In this process, up to 3% by weight of water is added to ...