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Quenching of High Entropy Alloys after Annealing
(2020)
The effect of cooling rate after annealing at 900 °C on the microstructure and hardness of high entropy alloys was investigated using two typical samples with the chemical composition of Co₁₆Cr₁₄.₅Fe₂₉Mn₁₁.₅Ni₂₉ and Co₁₁.₅Cr₇Fe₂₇Mn₂₇Ni₂₇(Nb₀.₀₈C₀.₅) (at%). The microstructural characterisation and hardness measurements were carried out by optical microscopy, scanning electron microscopy, wavelength-dispersive X-ray spectroscopy, electron back scattered diffraction, X-ray diffraction technique and Vickers hardness ...
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Comparative investigation of two-dimensional imaging methods and X-ray tomography in the characterization of microstructure
(2017-10-02)
The microstructural features of three different materials have been quantified by means of 2D image analysis and X-ray micro-computer tomography (CT) and the results were compared to determine the reliability of the 2D analysis in the material characterization. The 3D quantification of shrinkage pores and Fe-rich inclusions of an Al-Si-Cu alloy by X-ray tomography was compared with the statistical analysis of the 2D metallographic pictures and a significant difference in the results was found due to the complex ...
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Effect of Grain Statistics on Micromechanical Modeling: The Example of Additively Manufactured Materials Examined by Electron Backscatter Diffraction
(2020-02-21)
Micromechanical modeling is one of the prominent numerical tools for the prediction of mechanical properties and the understanding of deformation mechanisms of metals. As input parameters, it uses data obtained from microstructure characterization techniques, among which the electron backscatter diffraction (EBSD) technique allows us to understand the nature of microstructural features, that are usually described by statistics. Because of these advantages, the EBSD dataset is widely used for synthetic microstructure ...
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Effect of Friction Stir Processing on Microstructural, Mechanical, and Corrosion Properties of Al-Si12 Additive Manufactured Components
(2020-01-03)
Additive manufacturing (AM) is an advanced manufacturing process that provides the opportunity to build geometrically complex and highly individualized lightweight structures. Despite its many advantages, additively manufactured components suffer from poor surface quality. To
locally improve the surface quality and homogenize the microstructure, friction stir processing (FSP) technique was applied on Al-Si12 components produced by selective laser melting (SLM) using two different working media. The effect of FSP on ...
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Influence of complex geometries on the properties of laser-hardened surfaces
(2020-04-25)
Laser surface hardening provides for many advantages in terms of flexible production due to very localized and controlled energy input into the material. Laser processing offers the possibility to treat surfaces in order to locally strengthen the areas that are prone to fatigue cracking. It is well known that laser energy absorption depends on many parameters, e.g., the surface structure and the surface orientation. The incident angle of the laser beam plays a key role in this regard. When complex geometries like ...
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Effect of Post-Process Machining on Surface Properties of Additively Manufactured H13 Tool Steel
(2018-08-28)
Der Werkzeugstahl AISI H13 zeichnet sich durch einen hohen Verschleißwiderstand und eine gute Temperaturwechselbeständigkeit aus. Hauptanwendungsbereiche des H13 sind Druckguss- und Schmiedewerkzeuge. Die Verarbeitung von H13 durch additive Fertigungsverfahren, wie z. B. dem selektiven Laserschmelzen (selective laser melting, SLM), eröffnet neue Gestaltungsmöglichkeiten, wie z. B. die Integration interner Kühlkanäle, die es erlauben, das Einsatzverhalten der Werkzeuge zu verbessern. Aufgrund hoher Oberflächenrauheiten ...
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A Screening Approach for Rapid Qualitative Evaluation of Residual-Stress States – Application to Laser-Hardened Microalloyed Steel
(2019-06-11)
Surface hardening and compressive residual stresses are keys to superior part performance in numerous applications. In this context the development of advanced laser surface treatments for new materials and complex sample shapes is a time con-suming process. Eventually, determination of residual stress states by means of X-ray diffraction in the whole surface and subsurface region, respectively, is one of the main time consuming facors in terms of characterization. In many applications the provision of an adequate ...
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Martensite aging in ⟨001⟩ oriented Co₄₉ Ni₂₁ Ga₃₀ single crystals in tension
(2018-03-22)
Co–Ni–Ga high-temperature shape memory alloys (HT-SMAs) are well-known candidate materials for damping applications at elevated temperatures. Recent studies showed that upon heat treatment in stress-induced martensite under compressive loads transformation temperatures can be increased significantly, qualifying Co–Ni–Ga for HT-actuation. The increase in transformation temperatures is related to a change in chemical order recently validated via neutron diffraction experiments. Since SMAs show distinct tension–compression ...
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Electron beam welding of Fe–Mn–Al–Ni shape memory alloy: Microstructure evolution and shape memory response
(2017-07-03)
The present study reports on the impact of abnormal grain growth (AGG) on the microstructural evolution following electron beam (EB) welding of Fe–Mn–Al–Ni shape memory alloy (SMA). Polycrystalline sheet-like material was EB-welded and a cyclic heat treatment, studied in previous work, was conducted for inducing AGG and a bamboo-like microstructure, respectively. Optical and electron microscopy were carried out to characterize the prevailing microstructure upon cyclic heat treatment. For characterization of the ...
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Processing effects on tensile superelastic behaviour of Fe43.5Mn34Al15 ± XNi7.5∓X shape memory alloys
(2019)
Fe₄₃.₅Mn₃₄Al₁₅Ni₇.₅ was introduced in the current decade as a new superelastic alloy with great applicative potential due to: (i) superelastic behaviour over a thermal range of 200°C and (ii) recoverable strains up to 9.7 %. One of the key factors in enhancing the superelastic response of several shape memory alloys (SMAs) is the formation of an oligocrystalline structure, i.e. without triple junctions between grains, which is the result of an abnormal grain growth (AGG) process that can be induced by cyclic heat ...