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Aufsatz
Time-of-Flight Three Dimensional Neutron Diffraction in Transmission Mode for Mapping Crystal Grain Structures
(2017-08-25)
The physical properties of polycrystalline materials depend on their microstructure, which is the nano- to centimeter scale arrangement of phases and defects in their interior. Such microstructure depends on the shape, crystallographic phase and orientation, and interfacing of the grains constituting the material. This article presents a new non-destructive 3D technique to study centimeter-sized bulk samples with a spatial resolution of hundred micrometers: time-of-flight three-dimensional neutron diffraction (ToF ...
Aufsatz
Shape memory effect and superelasticity in high-strength FeNiCoAlTi single crystals hardened by nanoparticles
(2019-11-19)
For [001]-oriented single crystals of Fe-28Ni-17Co-11.5Al-2.5Ti (at %) alloy in tension, it was shown that particles of the γ’-phase with a size of 4–6 nm lead to the appearance of superelasticity, with a strain of εSE=4.5% and a shape memory effect of εSME=5.9%. Increasing the particle size to 10–12 nm reduces εSE to 3.6% and εSME to 3.5%. The paper discusses the causes of the influence of particle size on the reversible strain.
Aufsatz
Excellent superelasticity in a Co-Ni-Ga high-temperature shape memory alloy processed by directed energy deposition
(2020-04-30)
A Co-Ni-Ga high-temperature shape memory alloy has been additively manufactured by directed energy deposition. Due to the highly anisotropic microstructure, i.e. columnar grains featuring a strong near-⟨001⟩ texture in build direction, the as-built material is characterized by a very low degree of constraints and, thus, shows excellent superelasticity without conducting a post-process heat treatment. As characterized by in situ deformation testing and post-mortem microstructural analysis, additive manufacturing ...
Aufsatz
Novel Class of Rhenium Borides Based on Hexagonal Boron Networks Interconnected by Short B₂ Dumbbells
(2022-09-06)
Transition metal borides are known due to their attractive mechanical, electronic, refractive, and other properties. A new class of rhenium borides was identified by synchrotron single-crystal X-ray diffraction experiments in laser-heated diamond anvil cells between 26 and 75 GPa. Recoverable to ambient conditions, compounds rhenium triboride (ReB₃) and rhenium tetraboride (ReB₄) consist of close-packed single layers of rhenium atoms alternating with boron networks built from puckered hexagonal layers, which link ...
Aufsatz
A new method for microscale cyclic crack growth characterization from notched microcantilevers and application to single crystalline tungsten and a metallic glass
(2022-06-22)
The lifetime of most metals is limited by cyclic loads, ending in fatigue failure. The progressive growth of cracks ends up in catastrophic failure. An advanced method is presented for the determination of cyclic crack growth on the microscale using a nanoindenter, which allows the characterization of > 10,000 loading cycles. It uses focused ion beam fabricated notched microcantilevers. The method has been validated by cyclic bending metallic glass and tungsten microcantilevers. The experiments reveal a stable crack ...
Dissertation
Untersuchung von Gussporen in einer Aluminium-Gusslegierung mit der Computertomographie
(2022-04)
In dieser Arbeit wird das Schädigungsverhalten einer Aluminium-Gusslegierung anhand von zweidimensionalen und dreidimensionalen Verfahren untersucht. Dabei liegt das Hauptaugenmerk auf innenliegenden Gussdefekten wie Gas- und Schrumpfungsporen. Die Schädigungsentwicklung unter schwingender Belastung, sowie der Einfluss auf die Mikrostruktur und die mechanischen Eigenschaften sowie die Wechselwirkung verschiedener Gussdefekte werden dabei untersucht. Insbesondere wird der beim Versagensverhalten entscheidende Einfluss ...
Dissertation
The Fatigue and Corrosion Fatigue Behavior of Austenitic Stainless Steel AISI 304 after Deep Rolling at Various Temperatures
(2019-09)
The austenitic stainless steel AISI 304 was deep rolled at 20 °C (RTDR), -195 °C (CTDR), and 550 °C (HTDR). The deep rolling pressures used for each deep rolling temperature were 1.0, 1.7, and 2.4 bar. From microstructural investigation, the largest compressive residual stress field was found in RTDR, and the highest amount of martensitic content and plastic deformation were found in CTDR. The strain aging effect was only found in HTDR.
In the rotating bending fatigue tests, the strain aging effect after HTDR is ...
Aufsatz
Effect of Cell Morphology on Flexural Behavior of Injection-Molded Microcellular Polycarbonate
(2022-05-19)
The quantitative study of the structure and properties relationship in cellular materials is mostly limited to cell diameter, cell density, skin layer thickness, and cell size distribution. In addition, the investigation of the morphology is generally carried out in two dimensions. Therefore, the
interrelation between morphological properties and mechanical characteristics of the foam structure has remained in an uncertain state. In this study, during the physical foaming process, a foam morphology is locally created ...
Aufsatz
Mechanics of colloidal supraparticles under compression
(2021-10-13)
Colloidal supraparticles are finite, spherical assemblies of many primary particles. To take advantage of their emergent functionalities, such supraparticles must retain their structural integrity. Here, we investigate their size-dependent mechanical properties via nanoindentation. We find that the deformation resistance inversely scales with the primary particle diameter, while the work of deformation is dependent on the supraparticle diameter. We adopt the Griffith theory to such particulate systems to provide a ...
Aufsatz
On data-driven nonlinear uncertainty modeling: Methods and application for control-oriented surface condition prediction in hard turning
(2020-10-16)
In this article, two data-driven modeling approaches are investigated, which allow an explicit modeling of uncertainty. For this purpose, parametric Takagi-Sugeno multi-models with bounded-error parameter estimation and nonparametric Gaussian process regression are applied and compared. These models can for instance be used for robust model-based control design. As an application, the prediction of residual stresses during hard turning depending on the machining parameters and the initial hardness is considered.