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Cyclic Crack Growth in Chemically Tailored Isotropic Austenitic Steel Processed by Electron Beam Powder Bed Fusion
(2021-11-01)
The present study analyzes the cyclic crack propagation behavior in an austenitic steel processed by electron beam powder bed fusion (PBF-EB). The threshold value of crack growth as well as the crack growth behavior in the Paris regime were studied. In contrast to other austenitic steels, the building direction during PBF-EB did not affect the crack propagation rate, i.e., the crack growth rates perpendicular and parallel to the building direction were similar due to the isotropic microstructure characterized by ...
Aufsatz
Describing mechanical damage evolution through in situ electrical resistance measurements
(2023-02-27)
The fatigue properties of metallizations used as electrical conductors in flexible electronic devices have been thoroughly studied over the years. Most studies use time-intensive characterization methods to evaluate mechanical damage. For their ease of access, in situ electrical resistance measurements are often performed along with other characterization methods. However, the data are mostly used as an indicator of failure and a thorough analysis is usually missing. This work presents some deeper analysis methods ...
Aufsatz
Linking through-thickness cracks in metallic thin films to in-situ electrical resistance peak broadening
(2022-01-29)
Measurements of electrical resistance have been used extensively as a failure criterion in cyclically loaded conductive films. However, not much research has been performed on extracting additional information contained within such resistance data sets. This study shows that an increase in peak width evidences a transition from cracks bridging to through-thickness crack formation. A Au/Cr bilayer system on a polyimide substrate is used for data generation but the method is applicable to any material system where both ...
Aufsatz
Influence of Cu Addition and Microstructural Configuration on the Creep Resistance and Mechanical Properties of an Fe-Based α/α′/α″ Superalloy
(2023-01-14)
Introducing Cu nanoparticles is an effective mechanism for strengthening and toughening Fe-based materials such as ultra-high-strength steels. Herein, the effect of Cu on the mechanical properties of a novel Fe-based α/α′/α″ superalloy is studied. Compared to a Cu-free reference alloy, nanoindentation reveals an increase in hardness, which was associated with the formation of Cu nanoparticles. Both alloys show room temperature (RT) compressive plastic strain at maximum stress greater than 8%, irrespective of the ...
Aufsatz
Additive Manufacturing of 3D Luminescent ZrO2:Eu3+ Architectures
(2022-04-27)
Implementation of more refined structures at the nano to microscale is expected to advance applications in optics and photonics. This work presents the additive manufacturing of 3D luminescent microarchitectures emitting light in the visible range. A tailor-made organo-metallic resin suitable for two-photon lithography is developed, which upon thermal treatment in an oxygen-rich atmosphere allows the creation of silicon-free tetragonal (t-) and monoclinic (m-) ZrO₂. The approach is unique because the tailor-made ...
Aufsatz
Damage Tolerance Evaluation of E-PBF-Manufactured Inconel 718 Strut Geometries by Advanced Characterization Techniques
(2020-01-06)
By means of electron beam powder bed fusion (E-PBF), highly complex lightweight structures can be manufactured within short process times. Due to the increasing complexity of producible components and the entangled interplay of damage mechanisms, common bulk material properties such as ultimate tensile or fatigue strength are not sufficient to guarantee safe and reliable use in demanding applications. Within this work, the damage tolerance of E-PBF-manufactured Ni-based alloy Inconel 718 (IN 718) strut geometries ...
Aufsatz
Structural reorientation and compaction of porous MoS₂ coatings during wear testing
(2022-04-02)
Industrial upscaling frequently results in a different coating microstructure than the laboratory prototypes presented in the literature. Here, we investigate the wear behavior of physical vapor deposited (PVD) MoS2 coatings: A dense, nanocrystalline MoS2 coating, and a porous, prismatic-textured MoS2 coating. Transmission electron microscopy (TEM) investigations before and after wear testing evidence a crystallographic reorientation towards a basal texture in both samples. A basal texture is usually desirable due ...
Aufsatz
Tribological Performance of Additively Manufactured AISI H13 Steel in Different Surface Conditions
(2021-02-16)
Additive manufacturing of metallic tribological components offers unprecedented degrees of freedom, but the surface roughness of most as-printed surfaces impedes the direct applicability of such structures, and postprocessing is necessary. Here, the tribological performance of AISI H13 steel samples was studied. These were additively manufactured through laser powder bed fusion (L-PBF), also referred to as selective laser melting (SLM). Samples were tested in four different surface conditions: as-printed, polished, ...
Aufsatz
Elevated Temperature Mechanical Characteristics and Fracture Behavior of a Novel Beta Titanium Alloy
(2023-02-03)
In the present work, the elevated-temperature deformation characteristics and microstructural evolution of a Ti-5V-5Mo-5Cr-4Al alloy in solution-treatment conditions were studied under a tensile load at temperatures in the range of 25 to 550 °C and strain rates between 0.001 and 0.1 s-¹. The results obtained indicated that, essentially, dynamic recovery (DRV) was the dominant softening mechanism in the case of the regimes considered. An analysis based on transmission electron microscopy (TEM) and the assessment of ...
Aufsatz
Overmoulding of Additively Manufactured Titanium Inserts Using Polyoxymethylene (POM)—Evaluation of Bond Quality as a Function of Process Parameters
(2021-06-15)
Due to their process-induced porous surfaces, additively manufactured structures are not optimized for applications in which friction is a key factor. To improve the frictional properties of additively manufactured titanium inserts of various thicknesses, two tribologically optimized POM materials, which differ in terms of filler composition and contents, were used to overmould the inserts. The titanium inserts were manufactured in two different building directions, resulting in a variation in surface roughness. The ...