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Comparative investigation of two-dimensional imaging methods and X-ray tomography in the characterization of microstructure

The microstructural features of three different materials have been quantified by means of 2D image analysis and X-ray micro-computer tomography (CT) and the results were compared to determine the reliability of the 2D analysis in the material characterization. The 3D quantification of shrinkage pores and Fe-rich inclusions of an Al-Si-Cu alloy by X-ray tomography was compared with the statistical analysis of the 2D metallographic pictures and a significant difference in the results was found due to the complex morphology of shrinkage pores and Fe-rich particles. Furthermore, wood particles of a wood-plastic composite were measured by dynamic image analysis and X-ray tomography. Similar results were obtained for the maximum length of the particles, although the results of width differ considerably, which leads to a miscalculation of the particles aspect ratio. Finally, air voids of a foam concrete were investigated by the analysis of the 2D pictures in ImageJ and the results of the 2D circularity were compared with the values of the 3D elongation obtained by micro-computed tomography. The 3D analysis of the air voids in the foam concrete showed a more precise description of the morphology, although the 2D result are in good agreement with the results obtained by X-ray micro-tomography.

Sponsor
Initiative for the Development of Scientific and Economic Excel-lence (LOEWE) – Financial support of the special research project “Safer Materials”
Citation
In: Materials Testing Band 59 / Heft 10 (2017-10-02) , S. 829-836; eissn:0025-5300
Collections
@article{doi:10.17170/kobra-202304287912,
  author    ={Bacaicoa, Inigo and Lütje, Martin and Sälzer, Philipp and Umbach, Cristin and Brückner-Foit, Angelika and Heim, Hans-Peter and Middendorf, Bernhard},
  title    ={Comparative investigation of two-dimensional imaging methods and X-ray tomography in the characterization of microstructure},
  keywords ={660 and Mikroskopie and Aufnahme and Bildanalyse and Holz and Kunststoff and Verbundwerkstoff},
  copyright  ={https://rightsstatements.org/page/InC/1.0/},
  language ={en},
  journal  ={Materials Testing},
  year   ={2017-10-02}
}